************************************************************* DEHYDRO-TECH CORPORATION (Carver-Greenfield Process for Solvent Extraction of Wet, Oily Wastes) This vendor is participating in the EPA Superfund Innovative Technology Evaluation (SITE) Program. The following technology profile has been reproduced from the SITE Technology Profile document, 7th edition. The SITE profile has been supplemented by MVA Consulting Inc. using information obtained from the vendor or from other SITE publications, referenced at the end of this file. TECHNOLOGY DESCRIPTION: The Carver-Greenfield Process (C-G Process ) combines solvent extraction and dehydration technologies to separate wet, oily wastes into their constituent solid phase, water phase, and hydrocarbon-soluble indigenous oil phase. Waste is first mixed with a low cost hydro-carbon solvent, and the resultant slurry mixture is fed to an evaporator system that vaporizes water and initiates solvent extraction of the indigenous oil. Depending on the water content of the feed, single-effect or energy-saving multi-effect evaporators may be used. Next, the slurry of dried solids is treated in a multi-stage solvent extraction unit, where solids contact recycled solvent until the target amount of indigenous oil is removed. Finally, solids are centrifuged from the solvent, followed by "desolventizing," a step where resi-dual solvent is evaporated. The final solids pro-duct typically contains less than two percent water and less than one percent solvent. The spent solvent, which contains the extracted indi-genous oil, is distilled to separate the solvent for reuse later, and the oil for recovery or disposal. The C-G Process yields 1) a clean dry solid, 2) a water product virtually free of solids, indigenous oil, and solvent, and 3) the extracted indigenous oil which contains the hazardous hydrocarbon-soluble feed components. The C-G Process combination of water eva-poration and solvent extraction has the following advantages: 1) any emulsions initially present are broken and potential emulsion formation prevented; 2) solvent extraction is more efficient than with water present; and 3) the dry solids product is stabilized more readily if metals contamination is a concern. WASTE APPLICABILITY: The C-G Process can treat sludges, soils, sediments, and other water-bearing wastes containing hydrocarbon-soluble hazardous compounds, including polychlorinated biphenyls, polynuclear aromatic hydrocarbons, and dioxins. The process has been commercially applied to municipal wastewater sludge, paper mill sludge, rendering waste, pharmaceutical plant sludge, and other wastes. STATUS: The C-G Process was accepted into the SITE program in 1990. The pilot-scale SITE demonstration of this technology was completed in August 1991 at EPA's research facility in Edison, New Jersey. Spent petroleum drilling fluids from the PAB oil site in Abbe- ville, Louisiana, were used as process feed. The Applications Analysis Report (EPA/540/AR-92/002), Technology Demonstration Summary (EPA/540/SR-92/002), and Technology Evaluation Report (EPA/540/SR-92/002) were issued in 1992. DEMONSTRATION RESULTS: Based on spent drilling fluids, the C-G Process yielded the fol- lowing SITE demonstration results: > The process successfully separates a petroleum-oil contaminated sludge into its solid, indigenous oil, and water phases. No detectable levels of indigenous total petroleum hydrocarbons are present in the final solid product. > The final solid product is a dry powder similar to bentonite. A food-grade solvent comprises the bulk of the residual hydrocarbons on the solid. > Values for all metals and organics are well below the Resource Conservation and Recovery Act toxicity characteristic leaching procedure limits for characteristic hazardous wastes. > The resulting water product requires treatment due to the presence of small amounts of light organics and solvent. Normally, it may be disposed of at a local publicly owned treatment works. > A full scale C-G Process can treat drilling fluid wastes at technology-specific costs of $100 to $220 per ton of wet feed, exclusive of disposal costs for the residuals. Site-specific costs, which include the cost of residual disposal, are dependent on site characteristics and treatment objectives. FOR FURTHER INFORMATION: EPA PROJECT MANAGER: Laurel Staley U.S. EPA Risk Reduction Engineering Laboratory 26 West Martin Luther King Drive Cincinnati, OH 45268 513-569-7863 Fax: 513-569-7620 TECHNOLOGY DEVELOPER CONTACT: Theodore Trowbridge Dehydro-Tech Corporation 6 Great Meadow Lane East Hanover, NJ 07936 201-887-2182 Fax: 201-887-2548 __________________________________________________________ Sources of information in this profile: EPA Superfund Innovative Technology Evaluation Program Technology Profiles Seventh Edition, November 1994. EPA/540/R-94/526. *************************************************************